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¿ëµµ
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±Ô°Ý( ID × Length mm )
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Analytical
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2.0 × 150
(*)
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2.0 × 250
(*)
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4.6 × 150
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4.6 × 250
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Guard cartridge (3ea)
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4.0 × 10
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Semi-Prep
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10× 250
(*)
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20 × 250
(*)
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Semi-Prep Guard
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10 × 20
(*)
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Guard cartridge´Â
Cartridge Holder°¡ ÇÊ¿äÇÕ´Ï´Ù
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1. À̵¿»ó
Á¶¼º
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À̵¿»ó
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Á¶¼º
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Ethanol
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100 ~ 50% in MeOH, 2-PrOH or ACN
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Methanol
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100 ~ 50% in EtOH, 2-PrOH or ACN
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Acetonitrile
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100 ~ 80% in MeOH, 2-PrOH or ACN
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Hexane/EtOH
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99:1 ~ 50:50
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Hexane/2-PrOH
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99:1 ~ 50:50
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Hexane/MeOH
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99:1 ~ 95:5, MeOH 5% À̻󿡼´Â EtOH ÷°¡ 50:25:25
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MtBE/EtOH
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80:20 ~ 100:0
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Chloroform/Hexane
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25:75 ~ 100:0
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Dichloromethane/Hexane
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25:75 ~ 100:0
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Ethylacetate/Hexane
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20:80 ~ 70:30
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THF/Hexane
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10:90 ~ 50:50
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1,4-Dioxane/Hexane
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10:90 ~ 40:60
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Acetone/Hexane
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10:90 ~ 40:60
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-¾ËÄڿà ȥÇÕ¹°Àº Á¡¼ºÀÌ Å©¹Ç·Î
À¯¼ÓÀ» Á¶Á¤ÇÏ¿© ³·Àº ¾Ð·Â¿¡¼
»ç¿ëÇÏ¿© ÁֽʽÿÀ -MeOH¿Í HexaneÀÇ È¥ÇÕÀº MeOHÀÇ
Á¶¼ºÀÌ 5%°¡ ³Ñ¾î°¥ °æ¿ì, MeOH
´ë½Å¿¡, MeOH¿Í EtOHÀÇ 1:1
È¥ÇÕ¾×À»
»ç¿ëÇÏ¿© ÁֽʽÿÀ.
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2.
½Ã·áÁ¶Á¦ »ó±â ½Ã·á ¿ë¸Å¸¦ »ç¿ëÇϰí
0.45¥ìmÀÇ membrane filter·Î
¿©°úÇØ ÁֽʽÿÀ.
3. ¼¼Á¤
¹× º¸Á¸¹æ¹ý 100% DMF¸¦ 0.5§¢/min·Î 2½Ã°£
ÀÌ»ó Èê·ÁÁÖ°í ¿¡Åº¿ÃÀ» 0.5§¢/min·Î
30ºÐ ÀÌ»ó Èê·ÁÁØ ´ÙÀ½, ºÀÁö¸¶°³¸¦
ÇÑ ÈÄ, ½Ç¿ÂÇÏ¿¡¼ º¸Á¸ÇØ ÁֽʽÿÀ
4.
Regeneration »ç¿ë Àü¿¡ ¿¡Åº¿ÃÀ» 0.5§¢/min·Î
30ºÐ ÀÌ»ó Èê·ÁÁØ ´ÙÀ½, Çí»ê/¿¡Åº¿Ã
= 80/20(V/V)À¸·Î ¾ÈÁ¤È½ÃŲ
ÈÄ »ç¿ëÇÏ¿© ÁֽʽÿÀ
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